Module overview
This course follows on from CHEM1051 and teaches slightly more advanced basic skills, with the application of the Semester 1 skills and knowledge. More complex work-ups will be undertaken, with more emphasis on student input (or decision making) in the process. Students will also have the opportunity to learn how to use additional instrumentation (e.g. UV-Vis, Fluorescence Spectrometers).
Aims and Objectives
Learning Outcomes
Subject Specific Practical Skills
Having successfully completed this module you will be able to:
- Duplicate more advanced chemical laboratory procedures by following instructions
- Use previously learnt techniques to complete procedures with concise instructions
- Apply theoretical knowledge of basic techniques to choose appropriate conditions or techniques for parts of experiments
Syllabus
Lab skills to be developed
鈥pply previously learned skills (e.g. standard solutions) without detailed instructions
鈥elect appropriately sized equipment for procedures
鈥onsider the precision at which reagents, solvents etc need to be measured
鈥ake choices around experimental parameters including the scale at which procedures are carried out
鈥xpand range of spectroscopic techniques, with detailed instructions where new
鈥xplain the purpose of spectroscopic techniques that are applied
鈥ntisolvent crystallisation and base extraction
鈥se of RF to choose solvent mix for TLC to assess purity
鈥uild a colorimeter and modify supplied code to make time dependent measurements
Information and data skills
鈥rror estimation and questioning of 鈥渞easonableness鈥 with some guidance on when to apply
鈥nalyse data with some guidance and formulae given but without a step-wise breakdown
鈥lot graphs correctly with errors with minimal instruction
鈥eep an effective lab book without reference to a template
鈥ave/archive data with informative filenames and titles
鈥se chemical drawing software
鈥xtract specific information from a provided scientific paper or self-found sources
Personal and written skills
鈥lan timing of experimental work and data analysis based on lab script
鈥rite a concise lab report in a scientific style
鈥resent data in defined formats with informative labelling with minimal instruction
鈥articipate in a team working exercise
Learning and Teaching
Teaching and learning methods
Practical sessions, supported by pre-labs and some written assignments. 黑料社 skills and team skills delivered in some cases through separate sessions. This module formally carries zero effort since that is attributed to the three accompanying theory modules (3 x 45 h).
Type | Hours |
---|---|
Guided independent study | 20 |
Seminar | 10 |
Practical classes and workshops | 80 |
Preparation for scheduled sessions | 10 |
Total study time | 120 |
Assessment
Assessment strategy
Practical work, lab skills, written reports and presentations. This module formally carries zero CATS as the marks are attributed to the three accompanying theory modules.Summative
This is how we鈥檒l formally assess what you have learned in this module.
Method | Percentage contribution |
---|---|
Laboratory Report | 25% |
Laboratory Assignment | 25% |
Laboratory work and associated tasks | 50% |
Referral
This is how we鈥檒l assess you if you don鈥檛 meet the criteria to pass this module.
Method | Percentage contribution |
---|
Repeat Information
Repeat type: Internal